(E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate

Base Information

Chemical Name:(E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate
CAS No.:1209004-38-5
Molecular Formula:C₁₇H₁₇NO₃
Molecular Weight:283.327
Hs Code.:

Synonyms:(E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate

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Chemical Property of (E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate

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Technology Process of (E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate

There total 4 articles about (E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2406-04-4
4-(phenylimino)cyclohexa-2,5-dienone

: 140-88-5,9003-32-1
ethyl acrylate

: 1209004-38-5
(E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate

Guidance literature:: With palladium diacetate; Trimethylacetic acid; at 80 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.0c01929

Reference yield: 80.0%

: 2878-50-4,94664-72-9
α-(4-hydroxyphenyl)-N-phenyl nitrone

: 105-53-3
diethyl malonate

: 1209004-38-5
(E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate

Guidance literature:: diethyl malonate; With sodium ethanolate; for 0.0166667h; Microwave irradiation;

α-(4-hydroxyphenyl)-N-phenyl nitrone; for 0.0166667h; Microwave irradiation;
DOI:10.1080/00397910902985481

Reference yield:

: 106-51-4
p-benzoquinone

: 1209004-38-5
(E)-ethyl 3-((4-hydroxyphenyl)(phenyl)amino)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: copper diacetate; acetic acid / chlorobenzene / 3 h / 110 °C

2: palladium diacetate; Trimethylacetic acid / 12 h / 80 °C / Inert atmosphere; Sealed tube

With copper diacetate; palladium diacetate; acetic acid; Trimethylacetic acid; In chlorobenzene;
DOI:10.1021/acs.orglett.0c01929