C₃₉H₆₈O₁₁

Base Information

Chemical Name:C₃₉H₆₈O₁₁
CAS No.:1448001-78-2
Molecular Formula:C₃₉H₆₈O₁₁
Molecular Weight:712.962
Hs Code.:

C<sub>39</sub>H<sub>68</sub>O<sub>11</sub>

Synonyms:C₃₉H₆₈O₁₁

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Chemical Property of C₃₉H₆₈O₁₁

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Technology Process of C₃₉H₆₈O₁₁

There total 25 articles about C₃₉H₆₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₆₆O₁₁

: 1448001-78-2
C₃₉H₆₈O₁₁

Guidance literature:: With 10 wt% Pd(OH)2 on carbon; hydrogen; In methanol; ethyl acetate; at 20 ℃; for 5h; under 760.051 Torr;
DOI:10.1039/c3ob40552d

Reference yield:

: 176299-96-0
4-methoxyphenyl 4,6-O-benzylidene-β-D-galactopyranoside

: 1448001-78-2
C₃₉H₆₈O₁₁

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine / dichloromethane / 10 h / 0 - 20 °C

2.1: sodium cyanotrihydroborate; hydrogenchloride / tetrahydrofuran; diethyl ether / 2 h / 0 °C / Molecular sieve

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / -78 °C / Molecular sieve; Inert atmosphere

4.1: ammonium cerium (IV) nitrate / toluene; acetonitrile; water / 1 h / 0 °C

5.1: potassium carbonate / acetone / 3 h

6.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2.5 h / 0 - 20 °C / Molecular sieve

7.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 6 h / 40 °C

8.1: sodium methylate / methanol; dichloromethane / 3 h / 20 °C

8.2: Amberlite IR-120 resin (H form)

9.1: 10 wt% Pd(OH)2 on carbon; hydrogen / methanol; ethyl acetate / 5 h / 20 °C / 760.05 Torr

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; ammonium cerium (IV) nitrate; sodium cyanotrihydroborate; trimethylsilyl trifluoromethanesulfonate; 10 wt% Pd(OH)2 on carbon; hydrogen; sodium methylate; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile;
DOI:10.1039/c3ob40552d

Reference yield:

: 1238200-49-1
p-methoxyphenyl 2,3-O-acetyl-4,6-O-benzylidene-β-D-galactopyranoside

: 1448001-78-2
C₃₉H₆₈O₁₁

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium cyanotrihydroborate; hydrogenchloride / tetrahydrofuran; diethyl ether / 2 h / 0 °C / Molecular sieve

2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / -78 °C / Molecular sieve; Inert atmosphere

3.1: ammonium cerium (IV) nitrate / toluene; acetonitrile; water / 1 h / 0 °C

4.1: potassium carbonate / acetone / 3 h

5.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2.5 h / 0 - 20 °C / Molecular sieve

6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 6 h / 40 °C

7.1: sodium methylate / methanol; dichloromethane / 3 h / 20 °C

7.2: Amberlite IR-120 resin (H form)

8.1: 10 wt% Pd(OH)2 on carbon; hydrogen / methanol; ethyl acetate / 5 h / 20 °C / 760.05 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; ammonium cerium (IV) nitrate; sodium cyanotrihydroborate; trimethylsilyl trifluoromethanesulfonate; 10 wt% Pd(OH)2 on carbon; hydrogen; sodium methylate; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile;
DOI:10.1039/c3ob40552d