N-methyliminodiacetic acid boronate

Base Information

• Chemical Name: N-methyliminodiacetic acid boronate
• CAS No.: 1072960-68-9
• Molecular Formula: C₂₀H₂₂BNO₆
• Molecular Weight: 383.209
• Mol file: 1072960-68-9.mol

Synonyms:N-methyliminodiacetic acid boronate

Chemical Property of N-methyliminodiacetic acid boronate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-methyliminodiacetic acid boronate

There total 2 articles about N-methyliminodiacetic acid boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

4-(hydroxymethyl)phenylboronic acid MIDA ester (1072960-82-7) + 4-methoxybenzyl-2,2,2-trichloroacetimidate → N-methyliminodiacetic acid boronate (1072960-68-9)

Guidance literature:

With trifluorormethanesulfonic acid; In tetrahydrofuran; TfOH, THF, 0 -> 23°C, 5 h;

DOI:10.1021/ja8063759

Reference yield:

4-(hydroxymethyl)phenylboronic acid MIDA ester (1072960-82-7) + O-(4-methoxybenzyl)-trichloroacetimidate (89238-99-3) → N-methyliminodiacetic acid boronate (1072960-68-9)

Guidance literature:

With trifluorormethanesulfonic acid; In tetrahydrofuran; at 0 - 23 ℃; Inert atmosphere;

DOI:10.1021/ja8063759

Reference yield: 84.0%

N-methyliminodiacetic acid boronate (1072960-68-9) → C15H17BO4 (950590-42-8)

Guidance literature:

With water; sodium hydrogencarbonate; In methanol; at 23 ℃; for 3.5h; Inert atmosphere;

DOI:10.1021/ja8063759

upstream raw materials:

4-(hydroxymethyl)phenylboronic acid MIDA ester

O-(4-methoxybenzyl)-trichloroacetimidate

Downstream raw materials:

4-(hydroxymethyl)phenylboronic acid MIDA ester

C₁₅H₁₇BO₄