(2S,3R,4S,5R)-3-(2-bromoallyloxy)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran

Base Information

Chemical Name:(2S,3R,4S,5R)-3-(2-bromoallyloxy)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran
CAS No.:1612755-47-1
Molecular Formula:C₂₄H₃₇BrO₅
Molecular Weight:485.459
Hs Code.:

Synonyms:(2S,3R,4S,5R)-3-(2-bromoallyloxy)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4S,5R)-3-(2-bromoallyloxy)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran

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Technology Process of (2S,3R,4S,5R)-3-(2-bromoallyloxy)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran

There total 2 articles about (2S,3R,4S,5R)-3-(2-bromoallyloxy)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1612755-42-6
(2S,3R,4R,5R)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran-3-ol

: 513-31-5
2-bromoallyl bromide

: 1612755-47-1
(2S,3R,4S,5R)-3-(2-bromoallyloxy)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran

Guidance literature:: (2S,3R,4R,5R)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran-3-ol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

2-bromoallyl bromide; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1080/00397911.2013.871562

Reference yield:

: 130890-36-7
(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole

: 1612755-47-1
(2S,3R,4S,5R)-3-(2-bromoallyloxy)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / 6 h / 0 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

2.2: 3 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; sodium hydride; In tetrahydrofuran; water;
DOI:10.1080/00397911.2013.871562