(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole

Base Information

• Chemical Name: (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole
• CAS No.: 130890-36-7
• Molecular Formula: C₂₃H₃₆O₅
• Molecular Weight: 392.536

Synonyms:(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole

Chemical Property of (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole

Chemical Property:

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Technology Process of (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole

There total 1 articles about (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole (130890-35-6) → (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole (130890-36-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 6h; under 760 Torr; Yield given; Ambient temperature;

DOI:10.1016/S0040-4039(00)97772-4

Reference yield: 80.0%

methanol (67-56-1) + (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole (130890-36-7) → (3R,4R,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-tetrahydro-furan-3-ol (130890-37-8)

Guidance literature:

With Amberlite IR 120 H+; at 80 ℃; for 12h;

DOI:10.1016/S0040-4039(00)97772-4

Reference yield: 25.0%

methanol (67-56-1) + (3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-octyl-tetrahydro-furo[2,3-d][1,3]dioxole (130890-36-7) → (2R,3R,4R,5R)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran-3-ol (1612755-44-8) + (2S,3R,4R,5R)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran-3-ol (1612755-42-6)

Guidance literature:

With hydrogenchloride; In water; at 0 ℃; for 6h; Inert atmosphere;

DOI:10.1080/00397911.2013.871562

upstream raw materials:

(3aR,5R,6S,6aR)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-5-((Z)-oct-1-enyl)-tetrahydro-furo[2,3-d][1,3]dioxole

Downstream raw materials:

(3R,4R,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-tetrahydro-furan-3-ol

(3R,4S,5R)-2-Methoxy-4-(4-methoxy-benzyloxy)-5-octyl-3-prop-2-ynyloxy-tetrahydro-furan

(2R,3R,4R,5R)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran-3-ol

(2S,3R,4R,5R)-4-(4-methoxybenzyloxy)tetrahydro-2-methoxy-5-octylfuran-3-ol

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