({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene

Base Information

Chemical Name:({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene
CAS No.:1319722-51-4
Molecular Formula:C₂₀H₁₈O₆S₄
Molecular Weight:482.623
Hs Code.:

Synonyms:({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene

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Chemical Property of ({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene

Chemical Property:

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Technology Process of ({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene

There total 3 articles about ({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 111120-05-9
4-(phenylsulfonyl)but-2-yn-1-ol

: 1319722-51-4
({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene

Guidance literature:: With disulfur dichloride; triethylamine; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1055/s-0030-1260024

Reference yield:

: 33313-80-3
4-phenylsulfanyl-but-2-yn-1-ol

: 1319722-51-4
({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane

2: disulfur dichloride; triethylamine / diethyl ether / 1 h / 0 °C

With disulfur dichloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1055/s-0030-1260024

Reference yield:

: 5651-88-7
phenyl propargyl sulfide

: 1319722-51-4
({4-[({[4-(phenylsulfonyl)but-2-ynyl]oxy}dithio)oxy]but-2-ynyl}sulfonyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 2 h / -78 - 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane

3: disulfur dichloride; triethylamine / diethyl ether / 1 h / 0 °C

With disulfur dichloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1055/s-0030-1260024