(E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate

Base Information

Chemical Name:(E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate
CAS No.:1579273-96-3
Molecular Formula:C₂₄H₃₂O₄Si
Molecular Weight:412.601
Hs Code.:

Synonyms:(E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate

Suppliers and Price of (E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate

Chemical Property:

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Technology Process of (E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate

There total 5 articles about (E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1579273-95-2
1-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]prop-2-en-1-ol

: 108-24-7
acetic anhydride

: 1579273-96-3
(E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.01.016

Reference yield:

: 1205539-37-2
4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}benzaldehyde

: 1579273-96-3
(E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2014.01.016

Reference yield:

: 4049-39-2
4-benzyloxy-3-hydroxy-benzaldehyde

: 1579273-96-3
(E)-3-[4-(benzyloxy)-3-{(tert-butyldimethylsilyl)oxy}phenyl]allyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; dmap / dichloromethane / 20 °C

2: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2014.01.016