9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

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Chemical Name:9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine
CAS No.:1214733-00-2
Molecular Formula:C₃₁H₃₉N₉O₄Si
Molecular Weight:629.794
Hs Code.:

Synonyms:9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

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Chemical Property of 9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

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Technology Process of 9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

There total 1 articles about 9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1214732-99-6
9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

: 1214733-00-2
9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

Guidance literature:: 9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine; With water; trifluoroacetic acid; at 22 ℃; for 0.166667h; Inert atmosphere;

With sodium hydrogencarbonate; In water; ethyl acetate; Inert atmosphere;
DOI:10.1080/15257770903307151

Reference yield: 65.0%

: 4-(3-chlorophenyl)-2-(4-nitrophenoxy)-2-oxo-1,3,2-dioxaphosphorinane

: 1214733-00-2
9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

: 9-(3-azido-2-O-tert-butyldimethylsilyl-5-O-(4-(3-chlorophenyl)-2-oxo-1,3,2-dioxaphosphorinan-2-yl)-3-deoxy-β-D-ribofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

Guidance literature:: 9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine; With tert-butylmagnesium chloride; In tetrahydrofuran; at -40 ℃; for 0.416667h; Inert atmosphere;

4-(3-chlorophenyl)-2-(4-nitrophenoxy)-2-oxo-1,3,2-dioxaphosphorinane; In tetrahydrofuran; at -40 - 22 ℃; for 17h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water; Inert atmosphere;
DOI:10.1080/15257770903307151