9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

Base Information

• Chemical Name: 9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine
• CAS No.: 1214732-99-6
• Molecular Formula: C₃₇H₅₃N₉O₄Si₂
• Molecular Weight: 744.057
• Mol file: 1214732-99-6.mol

Synonyms:9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

Chemical Property of 9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

There total 1 articles about 9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

9-(2,5-bis-O-tert-butyldimethylsilyl-3-O-trifluoromethylsulfonyl-β-D-ribofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine (1214732-88-3) → 9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine (1214732-99-6)

Guidance literature:

With lithium azide; In N,N-dimethyl-formamide; at 22 ℃; for 3h; Inert atmosphere;

DOI:10.1080/15257770903307151

Reference yield: 75.0%

9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine (1214732-99-6) → 9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine (1214733-00-2)

Guidance literature:

9-(3-azido-2,5-bis-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine; With water; trifluoroacetic acid; at 22 ℃; for 0.166667h; Inert atmosphere;

With sodium hydrogencarbonate; In water; ethyl acetate; Inert atmosphere;

DOI:10.1080/15257770903307151

upstream raw materials:

9-(2,5-bis-O-tert-butyldimethylsilyl-3-O-trifluoromethylsulfonyl-β-D-ribofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine

Downstream raw materials:

9-(3-azido-2-O-tert-butyldimethylsilyl-3-deoxy-β-D-xylofuranosyl)-2-N-(N,N-dibenzylformamidino)guanine