2-benzoyl-3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

Base Information

Chemical Name:2-benzoyl-3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene
CAS No.:73153-31-8
Molecular Formula:C₁₉H₂₀FeOP₂
Molecular Weight:382.162
Hs Code.:

Synonyms:2-benzoyl-3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

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Chemical Property of 2-benzoyl-3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

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Technology Process of 2-benzoyl-3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

There total 2 articles about 2-benzoyl-3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 67887-86-9
3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

: 73153-31-8
2-benzoyl-3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

Guidance literature:: With benzoic acid anhydride; In dichloromethane; CF3SO3H was added to excess (C6H5CO)2O, stirred under N2 for 1 h, Fe-compd. was added dropwise, stirred for 1 h at room temp.; quenched with excess H2O and anhyd. Na2CO3, extd. with CH2Cl2, washed with H2O, dried over anhyd. Na2SO4, concd., chromd. with benzene, evapd., recrystd. from petroleum ether (b.p. 30-40°C) at -15°C, elem. anal.;
DOI:10.1016/S0020-1693(00)84491-6

Reference yield: 67.0%

: 67887-86-9
3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

: 98-88-4
benzoyl chloride

: 73153-31-8
2-benzoyl-3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene

Guidance literature:: benzoyl chloride; With aluminum (III) chloride; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

3,3',4,4'-tetramethyl-1,1'-diphosphaferrocene; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tetasy.2016.11.003