(E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone

Base Information

Chemical Name:(E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone
CAS No.:122567-33-3
Molecular Formula:C₂₀H₂₁NO₄
Molecular Weight:339.391
Hs Code.:

Synonyms:(E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone

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Chemical Property of (E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone

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Technology Process of (E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone

There total 3 articles about (E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 122567-28-6
(E)-1-(4-Methoxy-2,3,5,6-tetramethyl-phenyl)-3-phenyl-propenone

: 122567-33-3
(E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone

Guidance literature:: With nitric acid; acetic anhydride; at 0 ℃; for 2h;
DOI:10.1021/jo00278a011

Reference yield:

: 14337-37-2
2,3,5,6-tetramethylanisole

: 122567-33-3
(E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / CH₂Cl₂ / 2 h / 0 °C

2: 68 percent / 99percent HNO₃, acetic anhydride / 2 h / 0 °C

With aluminium trichloride; nitric acid; acetic anhydride; In dichloromethane;
DOI:10.1021/jo00278a011

Reference yield:

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 122567-33-3
(E)-1-(4-Methoxy-2,3,5-trimethyl-6-nitromethyl-phenyl)-3-phenyl-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / CH₂Cl₂ / 2 h / 0 °C

2: 68 percent / 99percent HNO₃, acetic anhydride / 2 h / 0 °C

With aluminium trichloride; nitric acid; acetic anhydride; In dichloromethane;
DOI:10.1021/jo00278a011