methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

Base Information

Chemical Name:methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate
CAS No.:197726-54-8
Molecular Formula:C₁₇H₂₄O₆
Molecular Weight:324.374
Hs Code.:

Synonyms:methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

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Chemical Property of methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

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Technology Process of methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

There total 1 articles about methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 134577-92-7
5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester

: 197726-54-8
methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.25h;
DOI:10.1016/S0968-0896(97)00090-4

Reference yield: 90.0%

: 197726-54-8
methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

: 197726-55-9
methyl-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}-4E-pentenoate

Guidance literature:: With dimethyl sulfoxide; at 180 ℃; for 0.5h;
DOI:10.1016/S0968-0896(97)00090-4

Reference yield:

: 197726-54-8
methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

: 197708-00-2
methyl-5-{4-hydroxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / DMSO / 0.5 h / 180 °C

2: 94 percent / H₂ / 10percent Pd/C / ethanol / 2 h / 25 °C / 760 Torr

3: 100 percent / pyridine hydrochloride / 4 h / 180 °C

4: 73 percent / H₂SO₄ / 16 h / Heating

With sulfuric acid; hydrogen; pyridine hydrochloride; dimethyl sulfoxide; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0968-0896(97)00090-4