5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester

Base Information

• Chemical Name: 5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester
• CAS No.: 134577-92-7
• Molecular Formula: C₁₇H₂₂O₆
• Molecular Weight: 322.358

Synonyms:5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester

Chemical Property of 5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester

Chemical Property:

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Technology Process of 5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester

There total 2 articles about 5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl 3-[1-(5-formyloxy-n-pentyl)oxy-4-(4-N,N-dimethylaminocarbonylbutanamido)benzen-2yl]propionate (134577-79-0) + methyl 4-(chlorocarbonyl)butyrate (1501-26-4) + 2-methoxy-benzenepropanoic acid (6342-77-4) → 5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester (134577-92-7)

Guidance literature:

With hydrogenchloride; aluminium chloride; In dichloromethane;

Reference yield:

→ 5[3-(2-carboxyethyl)-4-hydroxyphenyl]-5-oxopentanoic acid (134577-96-1) + 5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester (134577-92-7)

Guidance literature:

Reference yield: 84.0%

5-[4-methoxy-3-(2-methoxycarbonylethyl)-phenyl]-5-oxo-pentanoic acid methyl ester (134577-92-7) → methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate (197726-54-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.25h;

DOI:10.1016/S0968-0896(97)00090-4

upstream raw materials:

Methyl 3-[1-(5-formyloxy-n-pentyl)oxy-4-(4-N,N-dimethylaminocarbonylbutanamido)benzen-2yl]propionate

methyl 4-(chlorocarbonyl)butyrate

2-methoxy-benzenepropanoic acid

Downstream raw materials:

methyl-5-hydroxy-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

5-[3-(2-carboxyethyl)-4-hydroxyphenyl]pentanoic acid

methyl-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}pentanoate

methyl-5-{4-methoxy-3-[2-(methoxycarbonyl)ethyl]phenyl}-4E-pentenoate

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