N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine

Base Information

Chemical Name:N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine
CAS No.:86043-99-4
Molecular Formula:C₁₉H₂₅NO₄S
Molecular Weight:363.478
Hs Code.:

Synonyms:N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine

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Chemical Property of N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine

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Technology Process of N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine

There total 6 articles about N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 86043-98-3
2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanone O-(phenylmethyl)oxime

: 86043-99-4
N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine

Guidance literature:: With sodium cyanoborohydride; In acetic acid; for 7h; Ambient temperature;
DOI:10.1021/jo00170a034

Reference yield: 92.0%

: 86043-98-3
Toluene-4-sulfonic acid 3-benzyloxyimino-2,2-dimethyl-propyl ester

: 86043-99-4
N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine

Guidance literature:: With sodium cyanoborohydride; In acetic acid; for 16h; Ambient temperature;
DOI:10.1016/S0040-4039(00)81539-7

Reference yield:

: 18516-19-3
2,2-dimethyl-3-oxopropyl 4-methylbenzenesulfonate

: 86043-99-4
N-(phenylmethoxy)-2,2-dimethyl-3-<<(4-methylphenyl)sulfonyl>oxy>-1-propanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaOH / methanol / 4 h

2: 95 percent / NaCNBH₃ / acetic acid / 7 h / Ambient temperature

With sodium hydroxide; sodium cyanoborohydride; In methanol; acetic acid;
DOI:10.1021/jo00170a034