6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane

Base Information

Chemical Name:6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane
CAS No.:123075-98-9
Molecular Formula:C₁₄H₁₅ClO₃S
Molecular Weight:298.79
Hs Code.:

Synonyms:6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane

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Chemical Property of 6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane

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Technology Process of 6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane

There total 1 articles about 6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 123163-88-2
(1RS,4SR,5RS,6RS)-5-endo-chloro-6-exo-benzenesulfenyl-7-oxa-2-bicyclo<2.2.1>heptanone

: 107-21-1
ethylene glycol

: 123075-98-9
6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;
DOI:10.1021/jo00286a018

Reference yield: 90.0%

: 123075-98-9
6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane

: 123075-99-0
6-exo-(phenylsulfonyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid;
DOI:10.1021/jo00286a018

Reference yield:

: 123075-98-9
6-exo-(phenylsulfenyl)-5-endo-chloro-2,2-(ethylenedioxy)-7-oxabicyclo<2.2.1>heptane

: 123076-03-9
C₂₄H₂₅NO₆S

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 3-chloroperbenzoic acid

2: 90 percent / DBU / CHCl₃ / 0 °C

3: 85 percent / CH₂Cl₂ / 168 h / Ambient temperature

With 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform;
DOI:10.1021/jo00286a018