(R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one

Base Information

Chemical Name:(R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one
CAS No.:1454598-26-5
Molecular Formula:C₃₂H₃₈N₂O₄Si
Molecular Weight:542.75
Hs Code.:

Synonyms:(R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one

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Chemical Property of (R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one

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Technology Process of (R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one

There total 4 articles about (R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1454598-34-5
C₂₆H₂₄N₂O₄

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1454598-26-5
(R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one

Guidance literature:: With 1H-imidazole; In dichloromethane; at 40 ℃;
DOI:10.1002/chem.201204522

Reference yield:

: 33333-60-7
3-hydroxy-3-indolyl-2-oxindole

: 1454598-26-5
(R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 6'-hydroxy-9-amino-9-deoxy-epi-quinidine; C₄₈H₂₉O₄P / chloroform / 96 h / 0 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 0 °C

3: 1H-imidazole / dichloromethane / 40 °C

With 1H-imidazole; sodium tetrahydroborate; 6'-hydroxy-9-amino-9-deoxy-epi-quinidine; C₄₈H₂₉O₄P; In methanol; dichloromethane; chloroform;
DOI:10.1002/chem.201204522

Reference yield:

: 1454598-03-8
C₁₈H₁₆N₂O₂

: 1454598-26-5
(R)-3-((S)-2-(tert-butyldimethylsilyloxy)-1-(4-methoxybenzyloxy)ethyl)-3,3'-biindolin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 6'-hydroxy-9-amino-9-deoxy-epi-quinidine; C₄₈H₂₉O₄P / chloroform / 96 h / 0 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 0 °C

3: 1H-imidazole / dichloromethane / 40 °C

With 1H-imidazole; sodium tetrahydroborate; 6'-hydroxy-9-amino-9-deoxy-epi-quinidine; C₄₈H₂₉O₄P; In methanol; dichloromethane; chloroform;
DOI:10.1002/chem.201204522