1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide

Base Information

Chemical Name:1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide
CAS No.:658041-46-4
Molecular Formula:C₁₇H₁₂N₄O₄
Molecular Weight:336.307
Hs Code.:

Synonyms:1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide

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Chemical Property of 1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide

Chemical Property:

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Technology Process of 1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide

There total 4 articles about 1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 658041-39-5
2-formyl-3-[N'-(ω-chloroacetyl)-N'-(4-nitrophenyl)amino]indole

: 658041-46-4
1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 3h; Heating;
DOI:10.1023/A:1024887429776

Reference yield:

: 167954-19-0
3-[N-(4-nitrophenyl)amino]indole

: 658041-46-4
1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / POCl₃ / 3.5 h / 20 °C

2: water

3: 98 percent / Na₂CO₃ / toluene / 3 h / Heating

4: 84 percent / hydroxylamine hydrochloride; sodium acetate / ethanol / 3 h / Heating

With hydroxylamine hydrochloride; water; sodium acetate; sodium carbonate; trichlorophosphate; In ethanol; toluene; 1: Vilsmeier reaction;
DOI:10.1023/A:1024887429776

Reference yield:

: 2-diimethyliminomeethyl-3-[N-(4-nitrophenyl)amino]indole chloride

: 658041-46-4
1-(4-nitrophenyl)-2-oxo-1,2,3,6-tetrahydro[1,4]diazepino[6,5-b]indole 4-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: water

2: 98 percent / Na₂CO₃ / toluene / 3 h / Heating

3: 84 percent / hydroxylamine hydrochloride; sodium acetate / ethanol / 3 h / Heating

With hydroxylamine hydrochloride; water; sodium acetate; sodium carbonate; In ethanol; toluene;
DOI:10.1023/A:1024887429776