[(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide

Base Information

Chemical Name:[(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide
CAS No.:933987-39-4
Molecular Formula:C₃₃H₅₁O₃PSi₂
Molecular Weight:582.911
Hs Code.:

Synonyms:[(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide

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Chemical Property of [(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide

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Technology Process of [(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide

There total 1 articles about [(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1309604-83-8
C₂₁H₂₃O₃P

: 994-30-9
triethylsilyl chloride

: 933987-39-4
[(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide

Guidance literature:: With pyridine; dmap; In tetrahydrofuran; for 0.25h;

Reference yield:

: 933987-39-4
[(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide

: 1202355-91-6
C₂₁H₂₇⁽²⁾H₉O₃

: C₄₂H₆₇⁽²⁾H₉O₄Si₂

Guidance literature:: [(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

C₂₁H₂₇⁽²⁾H₉O₃; In tetrahydrofuran; hexane; at -78 ℃; for 2.5h;

Reference yield:

: 933987-39-4
[(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide

: 1202355-64-3
C₂₀H₂₈⁽²⁾H₆O₄

: C₄₁H₆₈⁽²⁾H₆O₅Si₂

Guidance literature:: [(2Z)-2-[(3S,5R)-5-bis[triethylsilyl]-2-methylenecyclohexylidene]-ethyl]diphenylphosphine oxide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

C₂₀H₂₈⁽²⁾H₆O₄; In tetrahydrofuran; hexane; at -78 ℃; for 2.5h;