methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

Base Information

Chemical Name:methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate
CAS No.:250602-41-6
Molecular Formula:C₃₃H₃₆N₂O₅
Molecular Weight:540.659
Hs Code.:

Synonyms:methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

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Chemical Property of methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

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Technology Process of methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

There total 11 articles about methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 250602-96-1
methyl 2,2-dimethyl-6-oxo-6-phenylhexanoate

: 250602-85-8
4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyamine

: 250602-41-6
methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

Guidance literature:: With sodium acetate; acetic acid; In ethanol; for 12h; Heating;
DOI:10.1248/cpb.51.138

Reference yield:

: 70969-99-2
1,1-Ethylenedioxy-4-iodo-1-phenylbutane

: 250602-41-6
methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / 0.33 h / -78 °C

1.2: HMPA / tetrahydrofuran / 3 h / -40 °C

2.1: 1 M aq. H₂SO₄ / acetone / 3 h / Heating

3.1: 47 percent / acetic acid; sodium acetate / ethanol / 12 h / Heating

With sulfuric acid; sodium acetate; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol; acetone;
DOI:10.1248/cpb.51.138

Reference yield:

: 103632-91-3
2-[2-(methoxycarbonyl)ethyl]-2-phenyl-1,3-dioxolane

: 250602-41-6
methyl (E)-2,2-dimethyl-6-{4-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 87 percent / lithium aluminum hydride / diethyl ether / 0.5 h / 0 °C

2.1: triethylamine / ethyl acetate / 0.5 h / 0 °C

3.1: NaI / acetone / 2 h / 60 °C

4.1: LDA / tetrahydrofuran / 0.33 h / -78 °C

4.2: HMPA / tetrahydrofuran / 3 h / -40 °C

5.1: 1 M aq. H₂SO₄ / acetone / 3 h / Heating

6.1: 47 percent / acetic acid; sodium acetate / ethanol / 12 h / Heating

With lithium aluminium tetrahydride; sulfuric acid; sodium acetate; acetic acid; triethylamine; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; ethanol; ethyl acetate; acetone;
DOI:10.1248/cpb.51.138