(S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid

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Chemical Name:(S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid
CAS No.:94732-87-3
Molecular Formula:C₂₇H₃₁N₇O₁₆
Molecular Weight:709.58
Hs Code.:

Synonyms:(S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid

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Chemical Property of (S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid

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Technology Process of (S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid

There total 12 articles about (S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55757-60-3
N-α-(tert-butoxycarbonyl)-L-lysine methyl ester

: 94732-87-3
(S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine

2: 20percent CF₃COOH / CH₂Cl₂

3: HCl / methanol

4: NaBH₃CN / methanol

5: KOD / D₂O

6: H₂, pyridine, CH₃COOH / Pd-C / methanol / pH 5.8

With pyridine; hydrogenchloride; potassium deuteroxide; hydrogen; sodium cyanoborohydride; acetic acid; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; water-d2;
DOI:10.1016/S0040-4039(00)95188-8

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 94732-87-3
(S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid

Guidance literature:: Multi-step reaction with 9 steps

1: diethyl ether

2: H₂ / Pd-C / methanol

3: pyridine

4: 20percent CF₃COOH / CH₂Cl₂

5: HCl / methanol

6: NaBH₃CN / methanol

7: KOD / D₂O

8: H₂, pyridine, CH₃COOH / Pd-C / methanol / pH 5.8

With pyridine; hydrogenchloride; potassium deuteroxide; hydrogen; sodium cyanoborohydride; acetic acid; trifluoroacetic acid; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; water-d2;
DOI:10.1016/S0040-4039(00)95188-8

Reference yield:

: 73548-77-3
Boc-L-Lys(Z)-OMe

: 94732-87-3
(S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: H₂ / Pd-C / methanol

2: pyridine

3: 20percent CF₃COOH / CH₂Cl₂

4: HCl / methanol

5: NaBH₃CN / methanol

6: KOD / D₂O

7: H₂, pyridine, CH₃COOH / Pd-C / methanol / pH 5.8

With pyridine; hydrogenchloride; potassium deuteroxide; hydrogen; sodium cyanoborohydride; acetic acid; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; water-d2;
DOI:10.1016/S0040-4039(00)95188-8