{2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester

Base Information

• Chemical Name: {2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester
• CAS No.: 263011-15-0
• Molecular Formula: C₁₅H₂₅N₃O₂
• Molecular Weight: 279.382

Synonyms:{2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester

Chemical Property of {2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester

Chemical Property:

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Technology Process of {2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester

There total 2 articles about {2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-(((benzyloxy)carbonyl)amino)ethyl 4-methylbenzenesulfonate (93407-96-6) + N,N',N'-trimethylenediamine (142-25-6) → {2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester (263011-15-0)

Guidance literature:

DOI:10.1021/jm991155o

Reference yield:

benzyl 2-hydroxyethylcarbamate (77987-49-6) → {2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester (263011-15-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: 93 percent / 48 h / 20 °C

With pyridine;

DOI:10.1021/jm0111088

Reference yield: 95.0%

{2-[(2-dimethylamino-ethyl)-methyl-amino]-ethyl}-carbamic acid benzyl ester (263011-15-0) → N′-(2-aminoethyl)-N′,N,N-trimethylethan-1,2-diamine (33451-85-3)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In methanol;

DOI:10.1021/jm991155o

upstream raw materials:

2-(((benzyloxy)carbonyl)amino)ethyl 4-methylbenzenesulfonate

N,N',N'-trimethylenediamine

benzyl 2-hydroxyethylcarbamate

Downstream raw materials:

N′-(2-aminoethyl)-N′,N,N-trimethylethan-1,2-diamine

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