2-(BENZYLOXYCARBONYLAMINO)ETHYL 4-METHYLBENZENESULFONATE

Base Information

Chemical Name:2-(BENZYLOXYCARBONYLAMINO)ETHYL 4-METHYLBENZENESULFONATE
CAS No.:93407-96-6
Molecular Formula:C17H19NO5S
Molecular Weight:349.408
Hs Code.:2924299090
Mol file:93407-96-6.mol

Synonyms:2-(BENZYLOXYCARBONYLAMINO)ETHYL 4-METHYLBENZENESULFONATE

Suppliers and Price of 2-(BENZYLOXYCARBONYLAMINO)ETHYL 4-METHYLBENZENESULFONATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-(((Benzyloxy)carbonyl)amino)ethyl4-methylbenzenesulfonate 95+%
5g
$ 602.00

American Custom Chemicals Corporation
2-(BENZYLOXYCARBONYLAMINO)ETHYL 4-METHYLBENZENESULFONATE 95.00%
5MG
$ 505.03

Alichem
2-(Benzyloxycarbonylamino)ethyl4-methylbenzenesulfonate
1g
$ 296.00

Alichem
2-(Benzyloxycarbonylamino)ethyl4-methylbenzenesulfonate
5g
$ 906.78

AK Scientific
2-(Benzyloxycarbonylamino)ethyl4-methylbenzenesulfonate
5g
$ 904.00

AK Scientific
2-(Benzyloxycarbonylamino)ethyl4-methylbenzenesulfonate
1g
$ 264.00

Total 5 raw suppliers

Chemical Property of 2-(BENZYLOXYCARBONYLAMINO)ETHYL 4-METHYLBENZENESULFONATE

Chemical Property:

PSA：93.57000
LogP:3.91190

Purity/Quality:

97% ^*data from raw suppliers

2-(((Benzyloxy)carbonyl)amino)ethyl4-methylbenzenesulfonate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(BENZYLOXYCARBONYLAMINO)ETHYL 4-METHYLBENZENESULFONATE

There total 4 articles about 2-(BENZYLOXYCARBONYLAMINO)ETHYL 4-METHYLBENZENESULFONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 98-59-9
p-toluenesulfonyl chloride

: 93407-96-6
2-(((benzyloxy)carbonyl)amino)ethyl 4-methylbenzenesulfonate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 15h; Inert atmosphere;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 93407-96-6
2-(((benzyloxy)carbonyl)amino)ethyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Huenig's base / CH₂Cl₂

2: 82 percent / pyridine

With pyridine; N-ethyl-N,N-diisopropylamine; In dichloromethane; 1: Acylation / 2: Tosylation;
DOI:10.1016/S0960-894X(00)00328-0

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 93407-96-6
2-(((benzyloxy)carbonyl)amino)ethyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DMAP; TEA / dioxane; H₂O / 12 h / 0 - 20 °C

2: 88 percent / DMAP; TEA / CH₂Cl₂ / 0 - 20 °C

With dmap; TEA; In 1,4-dioxane; dichloromethane; water;
DOI:10.1039/b312808c