2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid

Base Information

• Chemical Name: 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid
• CAS No.: 170029-58-0
• Molecular Formula: C₃₂H₄₇NO₆
• Molecular Weight: 541.728

Synonyms:2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid

Chemical Property of 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid

Chemical Property:

Purity/Quality:

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Technology Process of 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid

There total 4 articles about 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

bromoacetic acid methyl ester (96-32-2) + 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid) (170029-57-9) → 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid (170029-58-0)

Guidance literature:

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In toluene; at 40 - 50 ℃; for 0.25h;

DOI:10.1002/prac.19953370186

Reference yield:

4-methoxy-2-nitrophenol (1568-70-3) → 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid (170029-58-0)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / dioxane

2: dioxane / 0.25 h / Heating

3: 84 percent / NaOH, Tetrabutylammoniumiodid / toluene / 0.25 h / 40 - 50 °C

With sodium hydroxide; hydrogen; tetra-(n-butyl)ammonium iodide; palladium on activated charcoal; In 1,4-dioxane; toluene;

DOI:10.1002/prac.19953370186

Reference yield:

1,4-dimethoxy-2-nitrobenzene (89-39-4) → 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-anilid (170029-58-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 88 percent / LiI, quinoline / 0.25 h / 160 - 170 °C

2: H₂ / 10percent Pd/C / dioxane

3: dioxane / 0.25 h / Heating

4: 84 percent / NaOH, Tetrabutylammoniumiodid / toluene / 0.25 h / 40 - 50 °C

With quinoline; sodium hydroxide; hydrogen; tetra-(n-butyl)ammonium iodide; lithium iodide; palladium on activated charcoal; In 1,4-dioxane; toluene;

DOI:10.1002/prac.19953370186

upstream raw materials:

bromoacetic acid methyl ester

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(2-hydroxy-5-methoxyanilid)

4-methoxy-2-nitrophenol

1,4-dimethoxy-2-nitrobenzene

Downstream raw materials:

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-hydroxy-2-methoxycarbonylmethoxy-4-nitranilid)

(5-Amino-2-{2-[2,4-bis-(1,1-dimethyl-propyl)-phenoxy]-hexanoylamino}-4-hydroxy-phenoxy)-acetic acid methyl ester

2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-methoxy-2-methoxycarbonylmethoxy)-4-nitranilid

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