tris(3,5-diphenylpyrazolato)bis(1,2-dimethoxyathane)neodimium(III) - 1,2-dimethoxyethane (1/1)

Base Information

• Chemical Name: tris(3,5-diphenylpyrazolato)bis(1,2-dimethoxyathane)neodimium(III) - 1,2-dimethoxyethane (1/1)
• CAS No.: 936842-40-9
• Molecular Formula: C₄H₁₀O₂*C₅₃H₅₃N₆NdO₄
• Molecular Weight: 1072.4

Synonyms:tris(3,5-diphenylpyrazolato)bis(1,2-dimethoxyathane)neodimium(III) - 1,2-dimethoxyethane (1/1)

Chemical Property of tris(3,5-diphenylpyrazolato)bis(1,2-dimethoxyathane)neodimium(III) - 1,2-dimethoxyethane (1/1)

Chemical Property:

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Technology Process of tris(3,5-diphenylpyrazolato)bis(1,2-dimethoxyathane)neodimium(III) - 1,2-dimethoxyethane (1/1)

There total 1 articles about tris(3,5-diphenylpyrazolato)bis(1,2-dimethoxyathane)neodimium(III) - 1,2-dimethoxyethane (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

neodymium + 1,2-dimethoxyethane (110-71-4) + (η(1)-3,5-diphenylpyrazolato)trimethyltin(IV) → tris(3,5-diphenylpyrazolato)bis(1,2-dimethoxyathane)neodimium(III) - 1,2-dimethoxyethane (1/1) (936842-40-9) + hexamethyldistannane (661-69-8)

Guidance literature:

With Hg; In 1,2-dimethoxyethane; (N2), DME added to excess of Nd metal, Sn complex and 1-2 drops of Hg, stirred at room temp. for 5 d; filtered, concd., crystd. at -20°C, washed (hexane), dried (vac.), elem. anal.;

DOI:10.1002/ejic.200600045

upstream raw materials:

1,2-dimethoxyethane

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