2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine

Base Information

Chemical Name:2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine
CAS No.:1313867-34-3
Molecular Formula:C₁₉H₁₈N₂O₅S
Molecular Weight:386.428
Hs Code.:

Synonyms:2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine

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Chemical Property of 2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine

Chemical Property:

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Technology Process of 2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine

There total 3 articles about 2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1313867-25-2
5-benzyloxy-2-methylpent-1-en-3-yne

: 149552-43-2
[N-(nosyl)imino]phenyliodinane

: 1313867-34-3
2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine

Guidance literature:: With tetrakis(acetonitrile)copper(I) perchlorate; In acetonitrile; for 8h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c1cc11351h

Reference yield:

: 10605-68-2
4-methyl-4-penten-2-yn-1-ol

: 1313867-34-3
2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: tetrakis(acetonitrile)copper(I) perchlorate / acetonitrile / 8 h / Molecular sieve; Inert atmosphere

With tetrakis(acetonitrile)copper(I) perchlorate; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c1cc11351h

Reference yield:

: 78-80-8
2-methylbut-1-en-3-yne

: 1313867-34-3
2-(3-(benzyloxy)prop-1-ynyl)-2-methyl-1-(4-nitrophenylsulfonyl)aziridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.58 h / -78 - -20 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: tetrakis(acetonitrile)copper(I) perchlorate / acetonitrile / 8 h / Molecular sieve; Inert atmosphere

With n-butyllithium; tetrakis(acetonitrile)copper(I) perchlorate; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1039/c1cc11351h