Technology Process of C11H12O
There total 4 articles about C11H12O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C17H26OSi;
With
lithium hydroxide monohydrate;
In
N,N-dimethyl-formamide;
Inert atmosphere;
With
hydrogenchloride;
In
water; N,N-dimethyl-formamide;
Inert atmosphere;
DOI:10.1039/c3ob27491h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: titanium tetrachloride; zinc / tetrahydrofuran; dichloromethane; toluene / 0.08 h / 0 °C / Inert atmosphere
1.2: 1 h / Inert atmosphere
2.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / Inert atmosphere
4.2: Inert atmosphere
With
triethylsilane; n-butyllithium; lithium hydroxide monohydrate; boron trifluoride diethyl etherate; titanium tetrachloride; zinc;
In
tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c3ob27491h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / Inert atmosphere
2.2: Inert atmosphere
With
n-butyllithium; lithium hydroxide monohydrate;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob27491h
