{4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid

Base Information

Chemical Name:{4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid
CAS No.:719293-64-8
Molecular Formula:C₃₈H₃₀F₁₂O₆S₃
Molecular Weight:906.831
Hs Code.:

{4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid

Synonyms:{4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid

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Chemical Property of {4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid

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Technology Process of {4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid

There total 13 articles about {4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: {4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid diethyl ester

: 719293-64-8
{4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid

Guidance literature:: With sodium hydroxide; water; In ethanol; for 5h; Heating / reflux;

Reference yield:

: 719293-97-7
4,4'-diiodo-2,2'-bis(trifluoromethyl)diphenylsulfide

: 719293-64-8
{4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / palladium diacetate; triphenylphosphine / DMF (N,N-dimethyl-formamide) / 9 h / 110 °C / Heating / reflux

2.1: sodium hydroxide; water / methanol / 4 h / Heating / reflux

3.1: sodium periodate; hydrazine / ethanol; water / 5 h / 20 °C

4.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h

4.2: 48 h / 20 °C

5.1: triethylamine / dichloromethane / 20 °C

6.1: sodium tetrahydroborate / ISOPROPYLAMIDE / 0.5 h / 5 °C

6.2: 20 °C / Heating / reflux

7.1: sodium hydroxide; water / ethanol / 5 h / Heating / reflux

With sodium hydroxide; sodium tetrahydroborate; sodium periodate; water; triethylamine; hydrazine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; ISOPROPYLAMIDE; water;

Reference yield:

: 777-37-7
4-chloro-3-(trifluoromethyl)nitrobenzene

: 719293-64-8
{4-[3-(4-{4-[3-(4-carboxymethoxy-3-trifluoromethyl-phenylsulfanyl)-propyl]-2-trifluoromethyl-phenylsulfanyl}-3-trifluoromethyl-phenyl)-propylsulfanyl]-2-trifluoromethyl-phenoxy}-acetic acid

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium sulfide / water / 6 h / 100 °C / Heating / reflux

2.1: hydrazine / iron(III) chloride / ethanol / 32 h / Heating / reflux; Activated charcoal

3.1: hydrogenchloride; sodium nitrite / water / 0 °C

4.1: triethylamine / palladium diacetate; triphenylphosphine / DMF (N,N-dimethyl-formamide) / 9 h / 110 °C / Heating / reflux

5.1: sodium hydroxide; water / methanol / 4 h / Heating / reflux

6.1: sodium periodate; hydrazine / ethanol; water / 5 h / 20 °C

7.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h

7.2: 48 h / 20 °C

8.1: triethylamine / dichloromethane / 20 °C

9.1: sodium tetrahydroborate / ISOPROPYLAMIDE / 0.5 h / 5 °C

9.2: 20 °C / Heating / reflux

10.1: sodium hydroxide; water / ethanol / 5 h / Heating / reflux

With hydrogenchloride; sodium sulfide; sodium hydroxide; sodium tetrahydroborate; sodium periodate; water; triethylamine; hydrazine; sodium nitrite; iron(III) chloride; palladium diacetate; triphenylphosphine; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; ISOPROPYLAMIDE; water;