methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime

Base Information

Chemical Name:methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime
CAS No.:143954-96-5
Molecular Formula:C₁₆H₁₈N₆O₅
Molecular Weight:374.356
Hs Code.:

Synonyms:methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime

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Chemical Property of methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime

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Technology Process of methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime

There total 3 articles about methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 83269-21-0
α-aminopropiophenone oxime

: 121572-42-7
methyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 143954-96-5
methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: With triethylamine; In isopropyl alcohol; for 21h; Heating;
DOI:10.1021/jm00130a023

Reference yield:

: 121572-37-0
dimethyl (4-chloropyridine-2,6-diyl)bis

: 143954-96-5
methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / conc. H₂SO₄, red fuming HNO₃ / 1.75 h / 0 deg C to r.t.

2: 42 percent / Et₃N, H₂O / a) reflux, 9 h, b) r.t., 16 h

3: 74 percent / Et₃N / propan-2-ol / 21 h / Heating

With sulfuric acid; water; nitric acid; triethylamine; In isopropyl alcohol;
DOI:10.1021/jm00130a023

Reference yield:

: 121572-41-6
dimethyl (4-chloro-3-nitropyridine-2,6-diyl)bis

: 143954-96-5
methyl <6-amino-4-<(1-methyl-2-oxo-2-phenylethyl)amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / Et₃N, H₂O / a) reflux, 9 h, b) r.t., 16 h

2: 74 percent / Et₃N / propan-2-ol / 21 h / Heating

With water; triethylamine; In isopropyl alcohol;
DOI:10.1021/jm00130a023