N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide

Base Information

Chemical Name:N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide
CAS No.:126385-20-4
Molecular Formula:C₄₈H₆₀N₆O₁₂
Molecular Weight:913.037
Hs Code.:

Synonyms:N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide

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Technology Process of N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide

There total 5 articles about N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4422-95-1
1,3,5-benzene tris(carbonyl chloride)

: 126385-14-6
N-acetyl-N-(5-amino-3-oxapentyl)-O-benzylhydroxylamine

: 126385-20-4
N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide

Guidance literature:: With triethylamine; In dichloromethane; 0 deg C, 1 h, Rt, 2 h;

Reference yield:

: 90195-00-9
N-<(2,2,2-trichloroethoxy)carbonyl>-O-benzylhydroxylamine

: 126385-20-4
N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide

Guidance literature:: Multi-step reaction with 4 steps

2: 97 percent / dimethylformamide / 18 h / 120 °C

3: 40 percent aq. MeNH₂ / ethanol / 36 h / Ambient temperature

4: 90 percent / Et₃N / CH₂Cl₂ / 0 deg C, 1 h, Rt, 2 h

With triethylamine; methylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 126385-08-8
N-acetyl-O-benzyl-N-(5-bromo-3-oxapentyl)hydroxylamine

: 126385-20-4
N,N',N''-tris<5-acetyl(benzyloxy)amino-3-oxapentyl>benzene-1,3,5-tricarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / dimethylformamide / 18 h / 120 °C

2: 40 percent aq. MeNH₂ / ethanol / 36 h / Ambient temperature

3: 90 percent / Et₃N / CH₂Cl₂ / 0 deg C, 1 h, Rt, 2 h

With triethylamine; methylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;