1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide

Base Information

• Chemical Name: 1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide
• CAS No.: 83151-19-3
• Molecular Formula: C₈H₁₅NO₃S₂
• Molecular Weight: 237.344
• Mol file: 83151-19-3.mol

Synonyms:1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide

Chemical Property of 1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide

There total 5 articles about 1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-Acetylcysteine (7218-04-4,26117-28-2,616-91-1,7696-05-1) + 2-(((3-acetamido-4-methoxy-2-methyl-4-oxobutan-2-yl)disulfanecarbonyl)(methyl)amino)-N-methylethan-1-aminium trifluoroacetate → 1,3-dimethyl-2-imidazolidinone (80-73-9) + carbon oxide sulfide (463-58-1) + N,N'-bis(acetyl)cystine (5545-17-5,97247-12-6,139602-29-2) + C13H25N3O4S2*H(1+) + C13H22N2O6S3 + C13H22N2O6S4 + C13H22N2O6S5 + C16H28N2O6S5 + C16H28N2O6S6 + C16H28N2O6S3 (76480-10-9) + C16H28N2O6S4 (76480-11-0) + 1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide (83151-19-3)

Guidance literature:

With diethylenetriaminopentaacetic acid; In aq. buffer; at 37 ℃; pH=7.4;

DOI:10.1021/jacs.9b12180

Reference yield:

N-Acetylcysteine (7218-04-4,26117-28-2,616-91-1,7696-05-1) + 2-(((3-acetamido-4-methoxy-2-methyl-4-oxobutan-2-yl)disulfanecarbonyl)(methyl)amino)ethan-1-aminium trifluoroacetate → 1-methyl-2-imidazolidone (694-32-6) + carbon oxide sulfide (463-58-1) + methyl 2-acetamido-3-mercapto-3-methylbutanoate (39239-85-5) + N,N'-bis(acetyl)cystine (5545-17-5,97247-12-6,139602-29-2) + C13H22N2O6S2 + C12H23N3O4S2*H(1+) + C13H22N2O6S3 + C13H22N2O6S4 + C13H22N2O6S5 + C16H28N2O6S5 + C16H28N2O6S6 + C16H28N2O6S3 (76480-10-9) + C16H28N2O6S4 (76480-11-0) + 1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide (83151-19-3)

Guidance literature:

With diethylenetriaminopentaacetic acid; In aq. buffer; at 37 ℃; pH=7.4; pH-value;

DOI:10.1021/jacs.9b12180

Reference yield:

2-(((3-acetamido-4-methoxy-2-methyl-4-oxobutan-2-yl)disulfanecarbonyl)(methyl)amino)-N-methylethan-1-aminium trifluoroacetate → 1,3-dimethyl-2-imidazolidinone (80-73-9) + methyl 2-acetamido-3-mercapto-3-methylbutanoate (39239-85-5) + C16H28N2O6S5 + C16H28N2O6S6 + C16H28N2O6S3 (76480-10-9) + C16H28N2O6S4 (76480-11-0) + 1-Acetamido-1-(carbomethoxy)-2-methyl-2-propyl Hydrodisulfide (83151-19-3)

Guidance literature:

With diethylenetriaminopentaacetic acid; In aq. buffer; at 37 ℃; for 0.166667h; pH=7.4;

DOI:10.1021/jacs.9b12180

upstream raw materials:

N-Acetylcysteine

Downstream raw materials:

methyl 2-acetamido-3-<(2,4-dinitrophenyl)dithio>-3-methylbutanoate