(E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine

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Chemical Name:(E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine
CAS No.:626255-45-6
Molecular Formula:C₆₀H₉₄N₂O₇
Molecular Weight:955.416
Hs Code.:

Synonyms:(E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine

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Chemical Property of (E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine

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Technology Process of (E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine

There total 3 articles about (E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 626255-42-3
(E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylcarbamic acid tert-butyl ester

: 626255-45-6
(E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 2h; Heating;
DOI:10.1021/ja0211050

Reference yield:

: 65915-94-8
N-(tert-butoxycarbonyl)-1,6-diaminohexane hydrochloride

: 626255-45-6
(E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

2: 93 percent / p-toluenesulfonic acid / toluene / 2 h / Heating

With toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ja0211050

Reference yield:

: 273723-77-6
(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoic acid pentafluorophenyl ester

: 626255-45-6
(E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

2: 93 percent / p-toluenesulfonic acid / toluene / 2 h / Heating

With toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ja0211050