(E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester

Base Information

Chemical Name:(E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester
CAS No.:626255-47-8
Molecular Formula:C₆₅H₁₀₁N₃O₁₀
Molecular Weight:1084.53
Hs Code.:

(E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester

Synonyms:(E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester

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Chemical Property of (E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester

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Technology Process of (E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester

There total 4 articles about (E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 626255-45-6
(E,E)-N-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoyl}hexyldiamine

: 2949-22-6
Glycine ethyl ester isocyanate

: 626255-47-8
(E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester

Guidance literature:: In chloroform; at 20 ℃; for 0.5h;
DOI:10.1021/ja0211050

Reference yield:

: 65915-94-8
N-(tert-butoxycarbonyl)-1,6-diaminohexane hydrochloride

: 626255-47-8
(E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

2: 93 percent / p-toluenesulfonic acid / toluene / 2 h / Heating

3: 100 percent / CHCl₃ / 0.5 h / 20 °C

With toluene-4-sulfonic acid; triethylamine; In dichloromethane; chloroform; toluene;
DOI:10.1021/ja0211050

Reference yield:

: 273723-77-6
(E,E)-4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoic acid pentafluorophenyl ester

: 626255-47-8
(E,E)-6-{4-{4-(4-methyl-2,5-bis[(S)-2-methylbutoxy]styryl)-2,5-bis[(S)-2-methylbutoxy]styryl}-2,5-bis[(S)-2-methylbutoxy]benzoylamino}hexylureidoacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

2: 93 percent / p-toluenesulfonic acid / toluene / 2 h / Heating

3: 100 percent / CHCl₃ / 0.5 h / 20 °C

With toluene-4-sulfonic acid; triethylamine; In dichloromethane; chloroform; toluene;
DOI:10.1021/ja0211050