N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine

Base Information

• Chemical Name: N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine
• CAS No.: 479499-97-3
• Molecular Formula: C₆₅H₉₅N₃O₅
• Molecular Weight: 998.486
• Mol file: 479499-97-3.mol

Synonyms:N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine

Chemical Property of N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine

There total 2 articles about N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-nitrophenylhydrazone (100-16-3) + 4-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde (299204-61-8) → N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine (479499-97-3)

Guidance literature:

With acetic acid; In ethanol; for 4.5h; Heating;

DOI:10.1039/b200432a

Reference yield:

5,5-Dimethyl-2-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-[1,3]dioxane (299204-60-7) → N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine (479499-97-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / aq. CF₃CO₂H / CH₂Cl₂ / 5 h / 20 °C

2: 93 percent / AcOH / ethanol / 4.5 h / Heating

With acetic acid; trifluoroacetic acid; In ethanol; dichloromethane;

DOI:10.1039/b200432a

Reference yield: 57.0%

fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) + N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine (479499-97-3) → C125H94N2O3

Guidance literature:

N-(4-Nitro-phenyl)-N'-[1-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-meth-(E)-ylidene]-hydrazine; With pyridine; N-chloro-succinimide; In chloroform; at 0 - 20 ℃;

fullerene-C₆₀; With triethylamine; In toluene; for 0.666667h; microwave irradiation;

DOI:10.1039/b200432a

upstream raw materials:

4-nitrophenylhydrazone

4-((E)-2-{4-[(E)-2-(3,4,5-Tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde

5,5-Dimethyl-2-[4-((E)-2-{4-[(E)-2-(3,4,5-tris-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-[1,3]dioxane