Technology Process of C26H20F6N2O3
There total 5 articles about C26H20F6N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; copper diacetate;
In
1,2-dichloro-ethane;
at 20 ℃;
for 48h;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride / 1,4-dioxane / 72 h / 75 °C
2.1: tetrahydrofuran / 20 °C
3.1: hydrazine hydrate / ethanol / 48 h / 20 °C
4.1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
4.2: 0.17 h / 20 °C
5.1: pyridine; copper diacetate / 1,2-dichloro-ethane / 48 h / 20 °C / Molecular sieve
With
pyridine; hydrogenchloride; di-tert-butyl-diazodicarboxylate; copper diacetate; hydrazine hydrate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrahydrofuran / 20 °C
2.1: hydrazine hydrate / ethanol / 48 h / 20 °C
3.1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
3.2: 0.17 h / 20 °C
4.1: pyridine; copper diacetate / 1,2-dichloro-ethane / 48 h / 20 °C / Molecular sieve
With
pyridine; di-tert-butyl-diazodicarboxylate; copper diacetate; hydrazine hydrate; triphenylphosphine;
In
tetrahydrofuran; ethanol; 1,2-dichloro-ethane;