4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole

Base Information

Chemical Name:4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole
CAS No.:1225448-25-8
Molecular Formula:C₂₂H₂₇N₅O₃
Molecular Weight:409.488
Hs Code.:

Synonyms:4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole

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Chemical Property of 4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole

Chemical Property:

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Technology Process of 4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole

There total 2 articles about 4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-[4-acetyl-5-benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-di-methyl-5-morpholinopyrazole

: 1225448-25-8
4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole

Guidance literature:: With hydrazine hydrate; In tetrahydrofuran; at 20 - 25 ℃; for 14h;

Reference yield:

: 26990-69-2
1,3-dimethyl-5-morpholin-4-yl-1H-pyrazole-4-carbaldehyde

: 1208118-33-5
1,4-diacetyl-3-benzyl-3-methylpiperazine-2,5-dione

: 1225448-25-8
4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 14 h / Heating

2.1: hydrazine hydrate / tetrahydrofuran / 14 h / 20 - 25 °C

With hydrazine hydrate; lithium hexamethyldisilazane; In tetrahydrofuran; 1.1: Aldol Condensation;

Reference yield:

: 1225448-25-8
4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole

: 74-88-4
methyl iodide

: 1225447-32-4
4-[5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-di-methyl-5-morpholinopyrazole

Guidance literature:: 4-[5-Benzyl-5-methyl-3,6-dioxopiperazin-(2Z)-ylidenemethyl]-1,3-dimethyl-5-morpholinopyrazole; With sodium hydride; In paraffin oil (nujol); N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

methyl iodide; In paraffin oil (nujol); N,N-dimethyl-formamide; at 0 ℃; for 2h; Heating;