3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline

Base Information

Chemical Name:3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline
CAS No.:78018-84-5
Molecular Formula:C₂₇H₂₃N
Molecular Weight:361.486
Hs Code.:

3-Ethyl-2,4-diphenyl-5,6-dihydrobenzo<h>quinoline

Synonyms:3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline

Chemical Property:

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Technology Process of 3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline

There total 5 articles about 3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 78018-83-4
C₂₇H₂₃O⁽¹⁺⁾*BF₄^(1-)

: 78018-84-5
3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline

Guidance literature:: With ammonia;
DOI:10.1021/jo00332a013

Reference yield:

: 110-89-4
piperidine

: C₃₃H₂₈N⁽¹⁺⁾*BF₄^(1-)

: 4096-20-2
N-phenyl piperidine

: 78018-84-5
3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline

Guidance literature:: In chlorobenzene; at 100 ℃; Rate constant; Thermodynamic data; H, S, E_A, different C-3 substituents;

Reference yield:

: 495-40-9
propiophenone

: 78018-84-5
3-Ethyl-2,4-diphenyl-5,6-dihydrobenzoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / BF₃-OEt₂ / 4 h / 120 - 130 °C

2: 86 percent / conc. aq. NH₃ / methanol / 22 h / 20 - 25 °C

With ammonium hydroxide; boron trifluoride diethyl etherate; In methanol;