HO(CH₂)3NC₅H₂N(CH₃)2(CH₂)10NC₅H₃(CH₂)3OC₆H₄C(C₆H₄C(CH₃)3)3

Base Information

• Chemical Name: HO(CH₂)3NC₅H₂N(CH₃)2(CH₂)10NC₅H₃(CH₂)3OC₆H₄C(C₆H₄C(CH₃)3)3
• CAS No.: 1000591-84-3
• Molecular Formula: C₆₅H₈₇N₃O₂
• Molecular Weight: 942.425
• Mol file: 1000591-84-3.mol

Synonyms:HO(CH₂)3NC₅H₂N(CH₃)2(CH₂)10NC₅H₃(CH₂)3OC₆H₄C(C₆H₄C(CH₃)3)3

Chemical Property of HO(CH₂)3NC₅H₂N(CH₃)2(CH₂)10NC₅H₃(CH₂)3OC₆H₄C(C₆H₄C(CH₃)3)3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HO(CH₂)3NC₅H₂N(CH₃)2(CH₂)10NC₅H₃(CH₂)3OC₆H₄C(C₆H₄C(CH₃)3)3

There total 1 articles about HO(CH₂)3NC₅H₂N(CH₃)2(CH₂)10NC₅H₃(CH₂)3OC₆H₄C(C₆H₄C(CH₃)3)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

C65H71N3O2 (1000591-83-2) → HO(CH2)3NC5H2N(CH3)2(CH2)10NC5H3(CH2)3OC6H4C(C6H4C(CH3)3)3 (1000591-84-3)

Guidance literature:

With hydrogen; palladium dihydroxide; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1021/ja076570h

Reference yield: 67.0%

HO(CH2)3NC5H2N(CH3)2(CH2)10NC5H3(CH2)3OC6H4C(C6H4C(CH3)3)3 (1000591-84-3) + Pd(NC5H3(CONCH2C6H4OC6H12)2)(CH3CN) (1000591-75-2) → Pd(2+)*NC5H3(CONCH2C6H4OC6H12)2(2-)*HON2C10H5N(CH3)2C16H32OC37H43=Pd(NC5H3(C14H18O2N)2)(HON2C10H5N(CH3)2C16H32OC37H43) (1016638-32-6)

Guidance literature:

In dichloromethane; soln. Pd complex and ligand in CH2Cl2 were stirred at room temp. for 1 h;

DOI:10.1021/ja076570h

Reference yield: 25.0%

HO(CH2)3NC5H2N(CH3)2(CH2)10NC5H3(CH2)3OC6H4C(C6H4C(CH3)3)3 (1000591-84-3) + 4-[tris-(4-tert-butylphenyl)methyl]phenol (143998-20-3) → C102H129N3O2 (1000591-85-4)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1021/ja076570h

upstream raw materials:

C₆₅H₇₁N₃O₂

Downstream raw materials:

C₁₀₂H₁₂₉N₃O₂

Pd⁽²⁺⁾*NC₅H₃(CONCH₂C₆H₄OC₆H₁₂)2^(2-)*HON₂C₁₀H₅N(CH₃)2C₁₆H₃₂OC₃₇H₄₃=Pd(NC₅H₃(C₁₄H₁₈O₂N)2)(HON₂C₁₀H₅N(CH₃)2C₁₆H₃₂OC₃₇H₄₃)