N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester

Base Information

Chemical Name:N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester
CAS No.:1377924-50-9
Molecular Formula:C₁₅H₁₆N₂O₆S₂
Molecular Weight:384.434
Hs Code.:

Synonyms:N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester

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Chemical Property of N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester

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Technology Process of N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester

There total 2 articles about N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 321711-62-0
N-[2-(2-thienyl)ethyl]-3-nitrobenzenesulfonamide

: 96-32-2
bromoacetic acid methyl ester

: 1377924-50-9
N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.ejmech.2012.02.045

Reference yield:

: 121-51-7
3-nitrobenzenesulphonyl chloride

: 1377924-50-9
N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.02.045

Reference yield: 88.0%

: 1377924-50-9
N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester

: 1377923-99-3
N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine

Guidance literature:: N-[2-(2-thienyl)ethyl]-N-[(3-nitrophenyl)sulfonyl]glycine methyl ester; With sodium hydroxide; In methanol; for 1h; Reflux;

With hydrogenchloride; In water; at 20 ℃; pH=2;
DOI:10.1016/j.ejmech.2012.02.045