Technology Process of C27H31F3N4O8S
There total 5 articles about C27H31F3N4O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(+)-10-camphorsulfonic acid;
In
methanol;
at 20 ℃;
for 0.333333h;
DOI:10.1021/ol070376i
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 822 mg / sodium borohydride / ethanol / 0.17 h / 0 °C
2: 100 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran; toluene / 0.33 h / 20 °C
3: 100 percent / (+)-camphorsulfonic acid / methanol / 0.33 h / 20 °C
With
sodium tetrahydroborate; (+)-10-camphorsulfonic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; ethanol; toluene;
2: Mitsunobu reaction;
DOI:10.1021/ol070376i
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran; toluene / 0.33 h / 20 °C
2: 100 percent / (+)-camphorsulfonic acid / methanol / 0.33 h / 20 °C
With
(+)-10-camphorsulfonic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; toluene;
1: Mitsunobu reaction;
DOI:10.1021/ol070376i