C₁₁H₁₁FO₃

Base Information

• Chemical Name: C₁₁H₁₁FO₃
• CAS No.: 1347047-65-7
• Molecular Formula: C₁₁H₁₁FO₃
• Molecular Weight: 210.205
• Mol file: 1347047-65-7.mol

Synonyms:C₁₁H₁₁FO₃

Chemical Property of C₁₁H₁₁FO₃

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₁H₁₁FO₃

There total 2 articles about C₁₁H₁₁FO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C13H11Cl3FNO3 (1347046-85-8) → C11H11FO3 (1347047-65-7) + C11H10F2O2 (1347046-90-5)

Guidance literature:

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; α,α,α-trifluorotoluene; potassium fluoride [2.2.2]cryptand; (1S)-10-camphorsulfonic acid; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; diethyl ether; acetonitrile; at 20 ℃; for 0.333333h;

DOI:10.1021/ja2087213

Reference yield: 66.0%

3,4-butenediol (497-06-3,86161-40-2) + 4-fluorobenzoyl chloride (403-43-0) → C11H11FO3 (1347047-65-7)

Guidance literature:

With pyridine; In tetrahydrofuran; at 20 ℃; for 4.16667h;

DOI:10.1021/ja2087213

Reference yield: 90.0%

C11H11FO3 (1347047-65-7) + trichloroacetonitrile (545-06-2) → C13H11Cl3FNO3 (1347046-85-8)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/ja2087213

upstream raw materials:

C₁₃H₁₁Cl₃FNO₃

3,4-butenediol

4-fluorobenzoyl chloride

Downstream raw materials:

C₁₁H₁₀F₂O₂

C₁₁H₉FO₂

C₁₂H₁₃FO₃

C₁₃H₁₃FO₄