bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride

Base Information

Chemical Name:bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride
CAS No.:686740-94-3
Molecular Formula:C₂₉H₃₂NP₂*Cl
Molecular Weight:491.98
Hs Code.:

Synonyms:bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride

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Chemical Property of bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride

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Technology Process of bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride

There total 1 articles about bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 51-75-2
nitrogen mustard

: 65567-06-8,4541-02-0
lithium diphenylphosphide

: 686740-94-3
bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride

Guidance literature:: In tetrahydrofuran; at 0 - 5 ℃;
DOI:10.1016/S0022-328X(01)01341-9

Reference yield: 75.0%

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 686740-94-3
bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride

: 435269-16-2
[CoCl₂(bis(2-diphenylphosphinoethyl)methylamine)]

Guidance literature:: With NaOH; In ethanol; ligand hydrochloride was treated with 10 % NaOH, react. mixt. was extd. with toluene, dried over Na2SO4, solvent was evapd. to dryness, residue was dissolved in EtOH, dropped to soln. CoCl2 in EtOH, stirred at 20°C for 30 min and refluxed for 1 h; soln. was concd. in vacuo and cooled to -5°C, ppt. was filtered off, washed with cold EtOH and dried in vacuo at 60°C, recrystn. from CH2Cl2-petroleum ether; elem. anal.;
DOI:10.1016/S0022-328X(01)01341-9

Reference yield: 70.0%

: trichloro(phenylimido)bis(triphenylphosphine)rhenium(V)

: 686740-94-3
bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride

: 858127-42-1
cis,fac-Re(NPh)Cl₃(bis[(2-diphenylphosphino)ethyl]methylamine)*HCl

Guidance literature:: In acetonitrile; Re complex and aminodiphosphine hydrochloride in MeCN were refluxed for 4 h; react. mixt. was allowed to return to room temp., ppt. was filtered and washed with Et2O; elem. anal.;
DOI:10.1021/ic048486y