5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline

Base Information

• Chemical Name: 5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline
• CAS No.: 1429254-19-2
• Molecular Formula: C₁₈H₂₁NO₂
• Molecular Weight: 283.37

Synonyms:5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline

Chemical Property of 5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline

Chemical Property:

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Technology Process of 5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline

There total 1 articles about 5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C37H42N2O4 (1429254-27-2) → 5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline (1429254-19-2)

Guidance literature:

With hydrogenchloride; In tert-butyl methyl ether; water; at 20 ℃; for 18h;

DOI:10.1021/jm3014103

Reference yield: 62.0%

5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline (1429254-19-2) → 5-benzyloxy-7,8-dichloro-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline (1429254-21-6)

Guidance literature:

With thionyl chloride; acetic acid; In water; at 20 ℃; for 2h;

DOI:10.1021/jm3014103

Reference yield: 48.0%

6-chloro-N-(3-methoxy-phenyl)-nicotinamide (224817-08-7) + 5-benzyloxy-6-ethoxy-1,2,3,4-tetrahydro-isoquinoline (1429254-19-2) → C31H31N3O4 (1429254-03-4)

Guidance literature:

In isopropyl alcohol; for 48h; Reflux;

DOI:10.1021/jm3014103

upstream raw materials:

C₃₇H₄₂N₂O₄

Downstream raw materials:

C₃₁H₃₁N₃O₄

C₃₀H₃₀N₄O₃

C₃₁H₃₂N₄O₃

C₃₀H₂₈Cl₂N₄O₃

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