(2S,3S)-3-[(2S,3R,4S,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy]-2-methyl-3,4-dihydro-2H-pyran

Base Information

• Chemical Name: (2S,3S)-3-[(2S,3R,4S,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy]-2-methyl-3,4-dihydro-2H-pyran
• CAS No.: 212895-04-0
• Molecular Formula: C₃₀H₅₂O₅SeSi₂
• Molecular Weight: 627.871

Synonyms:(2S,3S)-3-[(2S,3R,4S,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy]-2-methyl-3,4-dihydro-2H-pyran

Chemical Property of (2S,3S)-3-[(2S,3R,4S,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy]-2-methyl-3,4-dihydro-2H-pyran

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Technology Process of (2S,3S)-3-[(2S,3R,4S,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy]-2-methyl-3,4-dihydro-2H-pyran

There total 1 articles about (2S,3S)-3-[(2S,3R,4S,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy]-2-methyl-3,4-dihydro-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

(2S,3S)-2-methyl-3,4-dihydro-2H-pyran-3-ol + Acetic acid (4S,5R,6R)-4,5-bis-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3-phenylselanyl-tetrahydro-pyran-2-yl ester → 3,4-bis-(tert-butyldimethylsilyl)-1,5-anhydro-2,6-dideoxy-D-arabino-hex-1-enitol (129830-33-7) + (2S,3S)-3-[(2S,3R,4S,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-methyl-3-phenylselanyl-tetrahydro-pyran-2-yloxy]-2-methyl-3,4-dihydro-2H-pyran (212895-04-0)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; dichloromethane; 1.) -78 deg C, 15 min, 2.) r.t., 5 min;

DOI:10.1002/(SICI)1521-3765(19980710)4:7<1324::AID-CHEM1324>3.0.CO;2-6

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