trans-bis(triphenylarsine)iodo[2-(trimethylsilylmethoxy)phenyl]palladium

Base Information

Chemical Name:trans-bis(triphenylarsine)iodo[2-(trimethylsilylmethoxy)phenyl]palladium
CAS No.:189276-40-2
Molecular Formula:C₄₆H₄₅As₂IOPdSi
Molecular Weight:1025.12
Hs Code.:

Synonyms:trans-bis(triphenylarsine)iodo[2-(trimethylsilylmethoxy)phenyl]palladium

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Chemical Property of trans-bis(triphenylarsine)iodo[2-(trimethylsilylmethoxy)phenyl]palladium

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Technology Process of trans-bis(triphenylarsine)iodo[2-(trimethylsilylmethoxy)phenyl]palladium

There total 3 articles about trans-bis(triphenylarsine)iodo[2-(trimethylsilylmethoxy)phenyl]palladium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 189276-36-6
(2-iodophenyloxymethyl)trimethylsilane

: 183314-77-4
Pd((C₆H₅CHCH)2CO)(As(C₆H₅)3)2

: 189276-40-2
((C₆H₅)3As)2IPd(C₆H₄OCH₂Si(CH₃)3)

Guidance literature:: In acetone; 23°C;
DOI:10.1021/om970085l

Reference yield: 65.0%

: 189276-36-6
(2-iodophenyloxymethyl)trimethylsilane

: [Pd₂(dibenzylideneacetone)3]*dibenzylideneacetone

: 603-32-7
triphenyl-arsane

: 189276-40-2
trans-bis(triphenylarsine)iodo[2-(trimethylsilylmethoxy)phenyl]palladium

Guidance literature:: In acetone; toluene; Ar-atmosphere; stirring Me2CO soln. of excess of AsPh3 and Pd-complex at23°C for 3 h, addn. of silane and MePh, heating at 40°C f or 17 h; filtration (Celite), evapn., trituration (Et2O); elem. anal.;
DOI:10.1021/om980157o