phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate

Base Information

Chemical Name:phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate
CAS No.:1375744-74-3
Molecular Formula:C₃₃H₃₂N₂O₅
Molecular Weight:536.627
Hs Code.:

Synonyms:phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate

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Chemical Property of phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate

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Technology Process of phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate

There total 6 articles about phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1375744-91-4
(2S)-2-[benzyl(phenoxycarbonyl)amino]propanoic acid

: 1375744-74-3
phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C

2: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

3: Dess-Martin periodane / dichloromethane

With oxalyl dichloride; sodium hydrogencarbonate; Dess-Martin periodane; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo3007144

Reference yield:

: 1375744-90-3
N-benzyl-N-[(2S)-1-chloro-1-oxopropan-2-yl]carbamate

: 1375744-74-3
phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

2: Dess-Martin periodane / dichloromethane

With sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo3007144

Reference yield:

: 7585-47-9,40297-69-6,65491-01-2
N-benzyl-(S)-alanine

: 1375744-74-3
phenyl N-benzyl-N-[(1S)-1-{[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}ethyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / water / 0 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C

3: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

4: Dess-Martin periodane / dichloromethane

With oxalyl dichloride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo3007144