C₅₁H₇₂N₃O₂₃PSi

Base Information

Chemical Name:C₅₁H₇₂N₃O₂₃PSi
CAS No.:1333414-30-4
Molecular Formula:C₅₁H₇₂N₃O₂₃PSi
Molecular Weight:1154.2
Hs Code.:

C<sub>51</sub>H<sub>72</sub>N<sub>3</sub>O<sub>23</sub>PSi

Synonyms:C₅₁H₇₂N₃O₂₃PSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₁H₇₂N₃O₂₃PSi

Chemical Property:

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Technology Process of C₅₁H₇₂N₃O₂₃PSi

There total 16 articles about C₅₁H₇₂N₃O₂₃PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₁H₇₂N₃O₂₂PSi

: 1333414-30-4
C₅₁H₇₂N₃O₂₃PSi

Guidance literature:: With tert.-butylhydroperoxide; In dichloromethane; acetonitrile; at -40 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol2021687

Reference yield:

: C₂₆H₃₅O₁₁N

: 1333414-30-4
C₅₁H₇₂N₃O₂₃PSi

Guidance literature:: Multi-step reaction with 13 steps

1.1: methanol; sodium methylate / 12 h / 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

3.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere

4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C

5.2: 20 °C

6.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere

7.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere

8.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 14 h / -78 - 20 °C / Inert atmosphere; Molecular sieve

9.1: hydrazinium monoacetate / methanol / 12 h / Inert atmosphere; Reflux

10.1: pyridine / 0 - 20 °C / Inert atmosphere

11.1: hydrogen; palladium(II) hydroxide; acetic acid / methanol / 48 h / 3375.34 Torr

12.1: 1H-tetrazole / dichloromethane; acetonitrile / 2 h / 0 °C

13.1: tert.-butylhydroperoxide / dichloromethane; acetonitrile / 1 h / -40 - 0 °C / Inert atmosphere

With pyridine; 1H-tetrazole; methanol; tert.-butylhydroperoxide; dmap; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium methylate; palladium(II) hydroxide; hydrazinium monoacetate; sodium hydride; toluene-4-sulfonic acid; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol2021687

Reference yield:

: C₁₈H₂₇NO₇

: 1333414-30-4
C₅₁H₇₂N₃O₂₃PSi

Guidance literature:: Multi-step reaction with 12 steps

1.1: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

2.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C

4.2: 20 °C

5.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere

6.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere

7.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 14 h / -78 - 20 °C / Inert atmosphere; Molecular sieve

8.1: hydrazinium monoacetate / methanol / 12 h / Inert atmosphere; Reflux

9.1: pyridine / 0 - 20 °C / Inert atmosphere

10.1: hydrogen; palladium(II) hydroxide; acetic acid / methanol / 48 h / 3375.34 Torr

11.1: 1H-tetrazole / dichloromethane; acetonitrile / 2 h / 0 °C

12.1: tert.-butylhydroperoxide / dichloromethane; acetonitrile / 1 h / -40 - 0 °C / Inert atmosphere

With pyridine; 1H-tetrazole; methanol; tert.-butylhydroperoxide; dmap; trimethylsilyl trifluoromethanesulfonate; hydrogen; palladium(II) hydroxide; hydrazinium monoacetate; sodium hydride; toluene-4-sulfonic acid; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol2021687