1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane

Base Information

Chemical Name:1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane
CAS No.:135646-65-0
Molecular Formula:C₃₆H₃₇N₅O₈
Molecular Weight:667.718
Hs Code.:

Synonyms:1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane

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Chemical Property of 1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane

Chemical Property:

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Technology Process of 1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane

There total 1 articles about 1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10314-06-4
4-phthalimidobutyryl chloride

: 132352-17-1
[2-(2-Amino-ethylamino)-ethyl]-carbamic acid benzyl ester; hydrochloride

: 135646-65-0
1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane

Guidance literature:: With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/jm00113a020

Reference yield:

: 135646-65-0
1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane

: [(S)-1-{[({[(S)-1-(2-{(4-Amino-butyryl)-[2-(4-amino-butyrylamino)-ethyl]-amino}-ethylcarbamoyl)-2-phenyl-ethylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamoyl}-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂, HOAc / 10percent Pd/C / ethanol / 25 °C / 760 Torr

2: DCC, HOBt

3: H₂NNH₂, HOAc / ethanol / Heating

With hydrogen; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; hydrazine; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00113a020

Reference yield:

: 135646-65-0
1-(benzyloxycarbonyl)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane

: 135646-70-7
1-(BOC-Tyr-Gly-Gly-Phe)-4,7-bis-(4-phthalimidobutyryl)-1,4,7-triazaheptane

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, HOAc / 10percent Pd/C / ethanol / 25 °C / 760 Torr

2: DCC, HOBt

With hydrogen; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00113a020