C₃₀H₂₈NP

Base Information

• Chemical Name: C₃₀H₂₈NP
• CAS No.: 1316251-04-3
• Molecular Formula: C₃₀H₂₈NP
• Molecular Weight: 433.533
• Mol file: 1316251-04-3.mol

Synonyms:C₃₀H₂₈NP

Chemical Property of C₃₀H₂₈NP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₈NP

There total 6 articles about C₃₀H₂₈NP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C30H31BNP → C30H28NP (1316251-04-3)

Guidance literature:

With diethylamine; at 50 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.tet.2011.05.075

Reference yield:

N-(Phenacyl)pyridinium (18413-03-1) → C30H28NP (1316251-04-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ammonium acetate

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -40 °C / Inert atmosphere

2.2: -40 - 22 °C / Inert atmosphere

3.1: diethylamine / 6 h / 50 °C / Inert atmosphere

With n-butyllithium; ammonium acetate; diethylamine; In tetrahydrofuran; hexane; 1.1: Krohnke reaction;

DOI:10.1016/j.tet.2011.05.075

Reference yield:

pyridine (110-86-1) → C30H28NP (1316251-04-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: iodine

2.1: ammonium acetate

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -40 °C / Inert atmosphere

3.2: -40 - 22 °C / Inert atmosphere

4.1: diethylamine / 6 h / 50 °C / Inert atmosphere

With n-butyllithium; ammonium acetate; iodine; diethylamine; In tetrahydrofuran; hexane; 2.1: Krohnke reaction;

DOI:10.1016/j.tet.2011.05.075

upstream raw materials:

pyridine

N-(Phenacyl)pyridinium

(+)-α-pinene

(1S)-pinocarvone