dimethyl [(S_S,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate

Base Information

• Chemical Name: dimethyl [(S_S,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate
• CAS No.: 1010692-99-5
• Molecular Formula: C₁₄H₂₃N₂O₆PS
• Molecular Weight: 378.386

Synonyms:dimethyl [(S_S,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate

Chemical Property of dimethyl [(S_S,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate

Chemical Property:

Purity/Quality:

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Technology Process of dimethyl [(S_S,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate

There total 1 articles about dimethyl [(S_S,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-(-)-N-[1-(4-nitrophenyl)ethylidene]-tert-butanesulfinamide (1010692-87-1) + Dimethyl phosphite (868-85-9) → C14H23N2O6PS + dimethyl [(SS,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate (1010692-99-5)

Guidance literature:

With potassium carbonate; In diethyl ether; at 20 ℃; for 20h;

DOI:10.1055/s-2007-990872

Reference yield: 84.0%

dimethyl [(SS,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate (1010692-99-5) → (R)-(+)-(1-amino-1-p-nitrophenyl)ethylphosphonic acid

Guidance literature:

dimethyl [(S_S,R)-(+)-1-(tert-butylsulfinylamino)-1-(4-nitrophenyl)ethyl]phosphonate; With hydrogenchloride; for 18h; Heating;

With methyloxirane; In ethanol; at 20 ℃; for 3h; Further stages.;

DOI:10.1055/s-2007-990872

upstream raw materials:

(S)-(-)-N-[1-(4-nitrophenyl)ethylidene]-tert-butanesulfinamide

Dimethyl phosphite

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