benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside
CAS No.:1264439-02-2
Molecular Formula:C₂₂H₂₅NO₅
Molecular Weight:383.444
Hs Code.:

Synonyms:benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside

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Chemical Property of benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside

There total 1 articles about benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1264439-47-5
C₃₁H₄₅NO₅Si

: 1264439-02-2
benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1016/j.tetlet.2010.11.078

Reference yield: 84.0%

: 1264439-02-2
benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside

: 1264439-05-5
benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-α-L-idopyranoside

Guidance literature:: With Wilkinson's catalyst; hydrogen; In ethanol; benzene; at 20 ℃; for 3h; under 760.051 Torr; stereoselective reaction;
DOI:10.1016/j.tetlet.2010.11.078

Reference yield:

: 1264439-02-2
benzyl 2-acetamido-3-O-benzyl-2,6-dideoxy-5,6-unhydro-α-D-glucopyranoside

: benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

: 1264439-12-4
benzyl 2-acetamido-3-O-benzyl-4-methoxyimino-2,4,6-trideoxy-α-L-idopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Wilkinson's catalyst; hydrogen / ethanol; benzene / 3 h / 20 °C / 760.05 Torr

2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 17 h / 20 °C

3: sodium hydrogencarbonate / methanol / 17 h / 65 °C

With Wilkinson's catalyst; hydrogen; sodium hydrogencarbonate; Dess-Martin periodane; In methanol; ethanol; dichloromethane; benzene;
DOI:10.1016/j.tetlet.2010.11.078